IFSOE 2026

Optimization of slot-die printing technology of self-assembling monolayers on NiOx surface for perovskite solar cells

Submitted: Jun 30, 2026

Abstract

The use of solution-processed self-assembled monolayers (SAMs) to passivate metal oxide thin films is an effective approach for high-performance perovskite solar cells. However, commonly used SAMs suffer from poor uniformity and wettability issues in ultrathin layers (<10 nm), leading to incomplete coverage. This limits their suitability for scalable slot-die coating. In this work, we synthesized a 4,4′,4″-nitrilotribenzoic acid (TPA-3C) that directly addressing the solvatophobicity and wetting mismatch of conventional carbazole-phosphonic acid SAMs under slot die processing. The three functionalities and star-shaped symmetry of the TPA-3C molecule make it possible to avoid orientation of the molecule with the non-anchoring groups toward the substrate during solution printing. Molecular engineering of a tri-functional triphenylamine core provides simultaneous control of wettability and surface potential, which translates into highly uniform SAM coverage and perovskite crystallization. We made a special focus on data fluctuations, standard deviation on recombination, transport and photoelectric performance of devices and modules. Slot die coating was implemented for both the SAM and CsFAPbI3 absorber in p i n devices and 12 cell modules, yielding champion power conversion efficiencies of 19.2% and 16.3%, respectively, together with relevant operational and thermal stability (>1000 h, ISOS-L-2). Correlating local non-uniform wetting spots with lifetime, dark saturation current, and temperature coefficients reveals that mitigating SAM-induced wetting defects is essential for scalable, stable perovskite photovoltaics.

Keywords

halide perovskites self-assembling monolayers passivation molecular design slot-die coating

References

  1. Yuchen Yuan et al. Energies 2025, 18(10), 2577.
  2. Yuchen Yuan et al. Energies 2025, 18(10), 2577.

Grant information

This work was supported by Russian Science Foundation (RSF) (project № 22-19-00812-P).